Title:
METHOD FOR PRODUCING SILYL SODIUM COMPOUND AND METHOD FOR DEOXIDIZING EPOXY COMPOUND
Document Type and Number:
Japanese Patent JP2020055769
Kind Code:
A
Abstract:
To construct a technique which can simply, efficiently and inexpensively synthesize a silyl sodium compound in a small number of processes and in a short time, especially to construct a technique which synthesizes a silyl sodium compound by using easily available reagents from a viewpoint of sustainability without using reagents which are difficult to handle and are toxic.SOLUTION: There is provided a method for synthesizing a silyl sodium compound comprising a step of reacting a dispersion obtained by dispersing a silyl halide compound or a disilane compound with sodium into a dispersion solvent, the silyl halide compound or the disilane compound as a starting compound, in a reaction solvent to obtain the silyl sodium compound. There is also provided a method for deoxidizing an epoxy compound comprising a step of reacting the silyl sodium compound obtained by synthesizing method of the silyl sodium compound with an epoxy compound to deoxidize the epoxy compound to stereoselectively produce an alkene compound.SELECTED DRAWING: Figure 1
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Inventors:
MURAKAMI YOSHIAKI
TSUBOUCHI GEN
TAKAI KAZUHIKO
ASAKO SOBI
TSUBOUCHI GEN
TAKAI KAZUHIKO
ASAKO SOBI
Application Number:
JP2018186776A
Publication Date:
April 09, 2020
Filing Date:
October 01, 2018
Export Citation:
Assignee:
KOBELCO ECO-SOLUTIONS CO LTD
UNIV OKAYAMA
UNIV OKAYAMA
International Classes:
C07F19/00; C07C1/247; C07C15/50; C07F1/04; C07F7/08
Attorney, Agent or Firm:
Patent business corporation r&c