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Title:
含フッ素ポリエーテルカルボン酸アミドの製造法
Document Type and Number:
Japanese Patent JP5381273
Kind Code:
B2
Abstract:
A fluorine-containing polyether carboxylic acid amide represented by the general formula: C n F 2n+1 O(C 3 F 6 O) m RfCONHAr, wherein Rf is a fluorocarbon group having 1 to 2 carbon atoms, Ar is a nitrogen-containing heterocyclic group, n is an integer of 1 to 3, and m is an integer of 10 to 30, is produced by reacting a fluorine-containing polyether carboxylic acid fluoride represented by the general formula: C n F 2n+1 O(C 3 F 6 O) m RfCOF, wherein Rf, n, and m are as defined above, with a nitrogen-containing heterocyclic amine compound represented by the general formula: ArNH 2 , wherein Ar is as defined above; wherein the reaction is carried out while a reaction temperature is first increased to 80 to 100°C, and then increased at a temperature increase rate that produces a temperature difference of 3 to 5°C after 48 hours.

Inventors:
Keisuke Kogane
Seiichiro Murata
Hideki Abe
Yusuke Takahashi
Application Number:
JP2009103036A
Publication Date:
January 08, 2014
Filing Date:
April 21, 2009
Export Citation:
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Assignee:
UNIMATEC CO.,LTD.
International Classes:
C08G65/333; C10M149/12
Domestic Patent References:
JP2049096A
JP10259173A
JP10176049A
JP2008266462A
Foreign References:
US5034525
Attorney, Agent or Firm:
Toshio Yoshida
Kazuko Yoshida