Title:
光学活性体の絶対配置決定法
Document Type and Number:
Japanese Patent JP4089181
Kind Code:
B2
Inventors:
Masato Matsugi
Nojima Masatomo
Yasuyuki Kita
Iyo Ito
Hagimoto rational
Nojima Masatomo
Yasuyuki Kita
Iyo Ito
Hagimoto rational
Application Number:
JP2001233118A
Publication Date:
May 28, 2008
Filing Date:
August 01, 2001
Export Citation:
Assignee:
Daiso Co., Ltd.
International Classes:
C07J3/00; C07B61/00; C07C33/20; C07C33/46; C07C35/21; C07C43/23; C07C211/27; C07C211/29; C07C211/30; C07C211/31; C07C229/36; C07J43/00
Domestic Patent References:
| JP2001261613A |
Other References:
YAMAGUCHI, S. et al.,Use of shift reagent with diastereomeric MTPA esters for determination of configuration and enantiomeric purity of secondary carbinols in 1H NMR spectroscopy,Tetrahedron,1976年,Vol.32,pp.1363-1367
SUGIMOTO, Y. et al.,Application of the MTPA Method to Deternination of Absolute Sterochemistry. The Hydroxymethyl-substituted Chiral Carbon of Carbocycles,Bull. Chem. Soc. Jpn.,1980年,Vol.53,p.3723-3724
DALE, J. et al.,Nuclear magnetic resonance enantiomer regents. Configurational correlations via nuclear magnetic resonance chemical shifts of diastereomeric mandelate, O-methylmandelate, and .alpha.-methoxy-.alpha.-trifluoromethylphenylacetate (MTPA) esters ,J Am Chem Soc,1973年 1月24日,Vol.95, No.2,p.1363-1367
MURATA, S. et al.,Novel regio-and stereo selectivesynthesis of 6-substituted pteridines and naturally occurring l-erythro-biopterin,Synthesis,1992年 3月30日,No.3,p.303-308
MATSUGI, M. et al.,Determination of absolute configuration of trans-2-arylcyclohexanols using remarkable aryl-induced 1H NMR shifts in diastereomeric derivatives,Tetrahedron Letters,2001年 9月24日,Vol.42,No.39,p.6903-6905
MATSUGI, M. et al.,Determination of stereochemistry and separation of diastereomeric derivatives of trans-2-pyridylcyclohexanols by extraction,Tetrahedron Letters,2001年11月 5日,Vol.42, No.45,p.8039-8042
MATSUGI, M. et al.,A novel determination method of the absolute configuration of 1-aryl-1-alkylalcohols and amines by an intramolecular CH/π shielding effect in 1H NMR,Tetrahedron Letters,2001年11月 5日,Vol.42, No.45,p.8019-8022
FEIGL, D. et al.,Resolution of trifluoromethylcabinols,J Org Chem,1968年,Vol.33, No.11,p.4242-4244
SUGIMOTO, Y. et al.,Application of the MTPA Method to Deternination of Absolute Sterochemistry. The Hydroxymethyl-substituted Chiral Carbon of Carbocycles,Bull. Chem. Soc. Jpn.,1980年,Vol.53,p.3723-3724
DALE, J. et al.,Nuclear magnetic resonance enantiomer regents. Configurational correlations via nuclear magnetic resonance chemical shifts of diastereomeric mandelate, O-methylmandelate, and .alpha.-methoxy-.alpha.-trifluoromethylphenylacetate (MTPA) esters ,J Am Chem Soc,1973年 1月24日,Vol.95, No.2,p.1363-1367
MURATA, S. et al.,Novel regio-and stereo selectivesynthesis of 6-substituted pteridines and naturally occurring l-erythro-biopterin,Synthesis,1992年 3月30日,No.3,p.303-308
MATSUGI, M. et al.,Determination of absolute configuration of trans-2-arylcyclohexanols using remarkable aryl-induced 1H NMR shifts in diastereomeric derivatives,Tetrahedron Letters,2001年 9月24日,Vol.42,No.39,p.6903-6905
MATSUGI, M. et al.,Determination of stereochemistry and separation of diastereomeric derivatives of trans-2-pyridylcyclohexanols by extraction,Tetrahedron Letters,2001年11月 5日,Vol.42, No.45,p.8039-8042
MATSUGI, M. et al.,A novel determination method of the absolute configuration of 1-aryl-1-alkylalcohols and amines by an intramolecular CH/π shielding effect in 1H NMR,Tetrahedron Letters,2001年11月 5日,Vol.42, No.45,p.8019-8022
FEIGL, D. et al.,Resolution of trifluoromethylcabinols,J Org Chem,1968年,Vol.33, No.11,p.4242-4244
Attorney, Agent or Firm:
Einosuke Kishimoto
Akira Watanabe
Norihiko Hibi
Kiyosue Yasuko
Akira Watanabe
Norihiko Hibi
Kiyosue Yasuko