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Title:
APPARATUS AND METHOD FOR PRODUCING AROMATIC POLYISOCYANATE
Document Type and Number:
Japanese Patent JP2004035490
Kind Code:
A
Abstract:

To provide an apparatus for producing an aromatic polyisocyanate by which the aromatic polyisocyanate can be obtained stably over a long period by preventing the formation of a fixed material in a heat exchanger and the plugging of a pipe in the heat exchanger in a phosgenation reaction in the production of the aromatic polyisocyanate; and to provide a method for producing the aromatic polyisocyanate.

The method for producing the aromatic polyisocyanate comprises a step for reacting an aromatic polyamine with phosgene, a step for cooling a vapor extracted from the reactor 1 by a heat exchanger 2, a step for separating the cooled fluid by a vapor-liquid separator 3 to a vapor component and a liquid component, and a step for refeeding the separated liquid component to the reactor 1. The aromatic amine is reacted with the phosgene in a solvent while spraying the solvent for preventing the aromatic polyisocyanate from dispersing from the reactor and flowing in the heat exchanger.


Inventors:
SAEKI TAKUYA
IZUKAWA TSUKURU
Application Number:
JP2002196179A
Publication Date:
February 05, 2004
Filing Date:
July 04, 2002
Export Citation:
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Assignee:
MITSUI TAKEDA CHEMICALS INC
International Classes:
C07C263/10; C07C265/14; (IPC1-7): C07C263/10; C07C265/14
Attorney, Agent or Firm:
Shunichiro Suzuki
Koji Makimura
Chihata Takahata
Toru Suzuki