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Title:
BATCH TYPE TRANSESTERIFICATION METHOD
Document Type and Number:
Japanese Patent JP2000302726
Kind Code:
A
Abstract:

To provide a batch type method for transesterification by which safe and stable operations can be carried out by preventing a part of an oligomer from scattering on a condenser, reflux pipe and a distillate discharging pipe during a reaction.

The calorific heat fed to a transesterifying vessel 1 is controlled according to the amount of an alkylene glycol staying in a rectifying column 7 during the transesterification in a method for leading a low-boiling point substance produced in the transesterification through the rectifying column 7 to a condenser 8, cooling and condensing the low-boiling point substance, distilling off the low-boiling point substance, controlling the temperature in the rectifying column 7 with a part of the resultant distillate as a refluxing liquid and carrying out the transesterification when an ester-forming derivative of an aromatic dicarboxylic acid and the alkylene glycol are subjected to the transesterification by a batch type method.


Inventors:
UCHIDA TOSHIO
IMAI SANJI
TOMOE SHIGEMICHI
MURAI MASUO
Application Number:
JP11069699A
Publication Date:
October 31, 2000
Filing Date:
April 19, 1999
Export Citation:
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Assignee:
NIPPON ESTER CO LTD
International Classes:
C07C67/03; C07C67/54; C07C69/80; (IPC1-7): C07C67/03; C07C67/54; C07C69/80