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Title:
EXTREME PRESSURE CLEANER BASED ON SULFIDED HYDROXYALKYLBENZOIC ACID/ALKYLPHENOL ALKALINE EARTH METAL SALT MIXTURE AND BEING EXCELLENT IN OIL SOLUBILITY AND ITS PRODUCTION
Document Type and Number:
Japanese Patent JPH11172273
Kind Code:
A
Abstract:

To obtain an extreme pressure cleaner being excellent oil solubility and based on a sulfided hydroxyalkylbenzoic acid/alkyl phenol alkaline earth metal salt mixture.

A reactant mixture comprising a phenol having a 4-6C aliphatic hydrocarbon side chain, a dihydric alcohol, and an alkaline earth metal reagent in an amount corresponding to a gram equivalent ratio of the phenol of 0.99 or below is reacted. Next, carbon dioxide is reacted with a distillation bottom obtained by distilling the reaction mixture until at least a major amount of the water is removed, and the amount of the dihydric alcohol is reduced to 0.6 mol or below per mol of the alkaline earth metal reagent. The obtained product is reacted with above 0.5 to below 4.0 mol, per mol of the alkaline earth metal reagent, elemental sulfur. A 16-36C higher fatty carboxylic acid is added in an amount of 0.1-1.0 mol, per mol of the alkaline earth metal reagent between the reactant preparation step and the sulfidation step.


Inventors:
IMAI JUN
YAMAOKA SHINJI
UEKI HIROYUKI
Application Number:
JP36251597A
Publication Date:
June 29, 1999
Filing Date:
December 15, 1997
Export Citation:
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Assignee:
COSMO SOGO KENKYUSHO KK
COSMO OIL CO LTD
International Classes:
C10M159/22; C10M177/00; C10N30/04; C10N40/25; C10N70/00; (IPC1-7): C10M159/22; C10M177/00
Attorney, Agent or Firm:
Sou Suga