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Title:
気体反応成分の供給制御方法および制御装置
Document Type and Number:
Japanese Patent JP4245298
Kind Code:
B2
Abstract:
A method comprises continuously supplying an alcohol to a pressurized reaction system, pressurizing carbon monoxide with a compressor 8 attached to a first feed line 22, for continuously supplying carbon monoxide to the reaction system via a second feed line 23 with a reference flow rate F, and converging excess carbon monoxide in the reaction system in the first feed line via a branched circulation line 24 for allowing to react alcohol with carbon monoxide. The reference flow rate F in the second feed line 23 is a total rate of a reference consumption flow rate Fcs in the reaction and a flow rate F1 in excess rate over a fluctuation consumption flow rate DELTA Fcv in the reaction system (F=Fcs+F1, F1> DELTA Fcv). According to the pressure fluctuation of the gaseous phase in the reaction system, the flow rate in the circulation line 24 is controlled to a flow rate Fr=F1- DELTA Fcv and the feed flow rate in the first feed line 22 is controlled to a flow rate Fsu=Fcs+ DELTA Fcv, for compensating a consumption rate variation in the reaction system with the feed flow rate of carbon monoxide. This ensures discharge inhibition of the gaseous reactant in a liquid phase pressurized reaction system (such as carbonylation reaction system) and effective utilization of the reactant for the reaction.

Inventors:
Hidehiko Nakajima
Hara Yoshiyuki
Manabu Yamada
Application Number:
JP2002051797A
Publication Date:
March 25, 2009
Filing Date:
February 27, 2002
Export Citation:
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Assignee:
Daicel Chemical Industry Co., Ltd.
International Classes:
B01J3/02; B01J3/00; B01J4/00; B01J4/02; B01J8/22; B01J10/00; B01J19/00; C07C51/12; C07C53/08
Domestic Patent References:
JP2001348202A
JP49006163B1
JP2000095723A
Foreign References:
WO1999065097A1
Attorney, Agent or Firm:
Mitsuo Kata