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Title:
LIQUID CRYSTAL COMPOUND AND ITS PREPARATION
Document Type and Number:
Japanese Patent JPS6013747
Kind Code:
A
Abstract:

NEW MATERIAL:The compound of formula I (R1 and R2 are 1W10C straight- chain alkyl provided that R1≠R2).

EXAMPLE: trans-4-Ethyl-4'-propyl-ONN-azoxybenzene.

USE: A liquid crystal composition suitable for forming a matrix-driving twisted nematic liquid crystal display.

PREPARATION: Ethyl bromide is added dropwise to magnesium in THF in nitrogen atmosphere to obtain ethylmagnesium bromide (a Grignard reagent). A THF solution of p-alkylaniline of formula II is added dropwise to the Grignard reagent under ice cooling and agitation. The resultant compound of formula III is stirred under ice cooling, and a THF solution of p-alkylnitrobenzene of formula IV is added dropwise to the compound, and the reaction mixture is separated and purified e.g. by column chromatography, etc. to obtain the objective compound of formula I .


Inventors:
SHIONOZAKI YOSHITAKE
MUKAI HIROSHI
Application Number:
JP12202683A
Publication Date:
January 24, 1985
Filing Date:
July 05, 1983
Export Citation:
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Assignee:
SUWA SEIKOSHA KK
International Classes:
C09K19/26; C07C67/00; C07C241/00; C07C291/08; G02F1/13; (IPC1-7): C09K19/26
Attorney, Agent or Firm:
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