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Patent Searching and Data


Title:
LOWLY SUBSTITUTED HYDROXYPROPYLCELLULOSE HIGHLY SOLUBLE IN AQUEOUS ALKALI SOLUTION AND PRODUCTION THEREOF
Document Type and Number:
Japanese Patent JPH06100601
Kind Code:
A
Abstract:

PURPOSE: To obtain a compound excellent in film formability, etc., by regulating the degree of hydroxypropylation of cellulose and the viscosity of a solution of the cellulose in an aqueous NaOH solution under given conditions each to a spicified volve.

CONSTITUTION: This compound has a degree of hydroxypropylation of 0.2-0.9 and a 2wt.% solution thereof in an 8wt.% aqueous NaOH solution has a viscosity (at 25°C) of 1,000cP or higher. It can be obtained preferably by reacting cellulose (e.g. linter) with 0.8-1.5mol of an alkali (e.g. NaOH) per mol of the anhydroglucose units in a medium consisting of 85-92wt.% t-butyl alcohol and water, the amount of the medium being 10-20 times by weight the amount of the cellulose, and reacting the resulting alkali cellulose with 1.1-5.0mol of propylene oxide per mol of the anhydroglucose units at 50-70°C for 2-5hr.


Inventors:
OOHASHI NOBUTOSHI
KIYOSE ATSUNOBU
Application Number:
JP24989192A
Publication Date:
April 12, 1994
Filing Date:
September 18, 1992
Export Citation:
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Assignee:
DAICEL CHEM
International Classes:
A61K9/36; A61K47/38; C08B11/00; C08B11/08; (IPC1-7): C08B11/00; A61K9/36; A61K47/38; C08B11/08
Attorney, Agent or Firm:
Kaoru Furuya (3 outside)