To provide an iodine-based polarizing film having high contrast by immersion-treating a PVA film in boric-acid containing aqueous solution with continuously pouring a sulfite into the boric-acid containing aqueous when the PVA film is immersion-treated.
A sulfite is added continuously or intermittently into boric-acid containing aqueous solution for immersion treatment. For composition of this boric-acid containing aqueous solution, weight ratio of water: boric acid: potassium iodine is usually about 100: (2-15):(2-20), preferably 100: (5-12):(5-15). Temperature of the boric-acid containing aqueous solution, for example 50°C, preferably, a range from 50°C to 85°C. In this case, as sulfite added to the boric-acid containing aqueous solution, for example, sulfite metal salt such as potassium sulfite or sodium sulfite is used. As a PVA film, a film produced from PVA having about 1,000-10,000 polymerization degree, preferably 1,500-5,000 is used.
HAYASHI SHIGETOSHI
KURATA NOBUYUKI
JPH02275905A | 1990-11-09 | |||
JPH1090517A | 1998-04-10 | |||
JPS55126202A | 1980-09-29 | |||
JPH0243504A | 1990-02-14 | |||
JPH1039137A | 1998-02-13 |