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Patent Searching and Data


Title:
METHOD AND APPARATUS FOR PRODUCING AROMATIC CARBOXYLIC ACID
Document Type and Number:
Japanese Patent JPH029839
Kind Code:
A
Abstract:

PURPOSE: To reduce power cost while increasing conversion efficiency and to obtain aromatic carboxylic acid of high quality by oxidizing aromatic alkyl in a liquid phase by using an oxidizing reactor enhanced in mixing characteristics.

CONSTITUTION: A stirrer 12 and the shaft 15 connected thereto are provided in a continuous stirring reaction tank 10 composed of a pressure-resistant container and an upper mixing element 13 composed of a disc turbine fitted with six blades and a lower mixing element 14 composed of a 6-blade turbine fitted with a pitch moving a liquid upwardly and outwardly from the shaft at a time of rotation are fixed to the shaft and a relatively narrow vertically arranged inner buffle 16 is provided. A mixture of a volatile aq. acid soln. medium containing aromatic alkyl and a catalyst is introduced into the reaction tank 10 from a conduit 25 and oxygen-containing gas is introduced into the reaction tank 10 from a gas introducing pipe 18 and a reaction product is taken out of a conduit 26. Heat generated by reaction is removed from the reaction mixture by the evaporation of the aq. solvent and a small amt. of aromatic alkyl and the evaporated substances are sent to a tower top condenser 20 and the condensed part is refluxed to the reaction tank 10.


Inventors:
MIYON KII RII
Application Number:
JP6234589A
Publication Date:
January 12, 1990
Filing Date:
March 16, 1989
Export Citation:
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Assignee:
AMOCO CORP
International Classes:
B01J8/22; C07B61/00; B01J19/00; B01J19/18; C07C51/265; C07C63/26; B01F7/00; B01F15/00; (IPC1-7): C07B61/00; C07C51/265; C07C63/26
Attorney, Agent or Firm:
Chika Takagi (2 outside)