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Title:
METHOD OF MODIFYING CARBOXYMETHYLCELLULOSE ETHER ALKALI SALT AND CARBOXYMETHYLCELLULOSE ETHER ALKALI SALT PREPARED THEREBY
Document Type and Number:
Japanese Patent JP3715343
Kind Code:
B2
Abstract:

PURPOSE: To prepare a carboxymethylcellulose ether alkali salt improved in water solubility by admitting an aqueous solution of the salt in a pressurized state into a metal powder layer to finely cut insoluble swollen gel particles.
CONSTITUTION: An aqueous solution or water-containing solvent solution of a carboxymethylcellulose ether alkali salt (hereinbelow abbreviated as CMC) is prepared. It is desirable that the concentration of CMC is about 1-20wt.%. This solution in a pressurized state is admitted into a metal powder layer (e.g. stainless steel powder layer) to finely cut the insoluble microgel contained in the solution. It is desirable that the metal powder has a protruded shape and a particle diameter of 10-5000μm. If the polymer leaving the metal powder layer is further admitted into a stainless steel filter, the effect of finely cutting microgels can be heightened and the water solubility of CMC can be improved.


Inventors:
Shoichi Nishizaki
Masago Okamoto
Application Number:
JP3256895A
Publication Date:
November 09, 2005
Filing Date:
February 21, 1995
Export Citation:
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Assignee:
Daiichi Kogyo Pharmaceutical Co., Ltd.
International Classes:
C08B11/12; (IPC1-7): C08B11/12
Domestic Patent References:
JP62096501A
JP62185701A
Attorney, Agent or Firm:
Masahiko Nishito