PURPOSE: To occlude hydrogen or deuterium in a hydrogen storage alloy with a high occlusion rate by using a closed electrolytic device and incorporating a specified amt. of sulfur compds. into an electroyte.
CONSTITUTION: A closed electrolytic device having a gas diffusion electrode as an anode 21 and hydrogen storage metal such as Pd as a cathode 22 is used. An inorg. or org. compd. contg. sulfur is incorporated into an electrolyte 23 by 100-700μm. Electrolysis is conducted at a hydrogen occlusion rate (H/Pd) of ≥0.97 or deuterium is occluded at a deuterium occlusion rate (D/Pd) of ≥0.90. When a sulfur compd. is added to the electrolyte 23, the desorption of the hydrogen atom occluded in the cathode 22 is suppressed, and the hydrogen occlusion rate is enhanced.
NAKADA TOSHIHIDE
TSUCHIDA YUMIKO
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