Title:
METHOD FOR PREPARING 1-HYDROPEROXY-16-OXABICYCLO[10.4.0]HEXADECANE
Document Type and Number:
Japanese Patent JP2011105762
Kind Code:
A
Abstract:
To provide a method for preparing 1-hydroperoxy-16-oxabicyclo[10.4.0]hexadecane (DDP-OOH).
The method for preparing 1-hydroperoxy-16-oxabicyclo[10.4.0]hexadecane (DDP-OOH) includes reacting 13-oxabicyclo[10.4.0]hexadec-1(12)-ene (DDP) with hydrogen peroxide in a diluent in the presence of a strong acid. The diluent has a pKa value of ≥4.5 and the strong acid has that of ≤1.5. After the reaction has taken place, the strong acid is neutralized with at least 0.9 molar equivalent of a base.
Inventors:
LAMBRECHT STEFAN
WERNER MARKUS
TOPP HANS-JUERGEN
RICHTER NORBERT
KUHN WALTER
WERNER MARKUS
TOPP HANS-JUERGEN
RICHTER NORBERT
KUHN WALTER
Application Number:
JP2011033022A
Publication Date:
June 02, 2011
Filing Date:
February 18, 2011
Export Citation:
Assignee:
SYMRISE GMBH & CO KG
International Classes:
C07D313/00; C07D311/94; C07D315/00
Domestic Patent References:
| JPS548677B1 | 1979-04-17 | |||
| JPH03167295A | 1991-07-19 |
Foreign References:
| CH582169A5 | 1976-11-30 |
Attorney, Agent or Firm:
Sadao Kumakura
Atsushi Hakoda
Kenji Asai
Shunichiro Mashiba
Atsushi Hakoda
Kenji Asai
Shunichiro Mashiba
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