Title:
METHOD FOR PRODUCING 4,4'-DICARBOXY-2,2'-BIPYRIDINE
Document Type and Number:
Japanese Patent JP2006206516
Kind Code:
A
Abstract:
To provide an industrially advantageous method for producing a high purity 4,4'-dicarboxy-2,2'-bipyridine.
The invention relates to the method for producing 4,4'-dicarboxy-2,2'-bipyridine comprising a coupling reaction of 2-halogeno-pyridines expressed by formula (1) in a basic condition, and then adjusting pH of the obtained reaction mixture with an acid to 4-6 to precipitate the 4,4'-dicarboxy-2,2'-bipyridine. The invention relates to the method for purifying 4,4'-dicarboxy-2,2'-bipyridine containing isonicotinic acid comprises preparation of a basic aqueous solution of the 4,4'-dicarboxy-2,2'-bipyridine, precipitation of the 4,4'-dicarboxy-2,2'-bipyridine by adjusting pH of the basic aqueous solution with an acid to 4-6.
Inventors:
SHIMADA MASATERU
Application Number:
JP2005021677A
Publication Date:
August 10, 2006
Filing Date:
January 28, 2005
Export Citation:
Assignee:
KOEI CHEMICAL CO
International Classes:
C07D213/803
Domestic Patent References:
JP2002513003A | 2002-05-08 | |||
JPH11309377A | 1999-11-09 |
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