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Title:
METHOD OF PRODUCING CATALYST FOR PRODUCING METHACRYLIC ACID
Document Type and Number:
Japanese Patent JP2012236186
Kind Code:
A
Abstract:

To provide a method of producing catalyst for producing methacrylic acid by which methacrolein is subjected to gas phase contact oxidation by molecular oxygen to produce the methacrylic acid at high yield.

In a method of producing catalyst for producing methacrylic acid including: (a) a preparation step of preparing aqueous slurry or mixture solution containing a catalyst component; (b) a drying step of drying the aqueous slurry or the mixture solution to obtain dried substance particles; (c) a shaping step of shaping the dried substance particles to obtain a shaped product; and (d) a heat treatment step of subjecting the shaped product to heat treatment. A value of a median size (d50: unit μm) of the dried substance particles is in a range of d50≤60, a value d10/d50 obtained by dividing a value of a particle size (d10: unit μm) corresponding to 10% of cumulative frequency distribution of the dried substance particles by d50 is in a range of 0.41≤d10/d50≤0.79, and a value d90/d50 obtained by dividing a value of a particle size (d90: unit μm) corresponding to 90% of the cumulative frequency distribution of the dried substance particles by d50 is in a range of 1.21≤d90/d50≤1.89.


Inventors:
TAGAWA YUICHI
KITAZONO KENICHI
KATO HIROKI
FUJITA TSUTOMU
KONDO MASAHIDE
Application Number:
JP2011266626A
Publication Date:
December 06, 2012
Filing Date:
December 06, 2011
Export Citation:
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Assignee:
MITSUBISHI RAYON CO
International Classes:
B01J27/199; B01J37/08; C07C51/235; C07C57/055; C07B61/00