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Title:
METHOD FOR PRODUCING FATTY ACID ESTER, AND BIODIESEL FUEL
Document Type and Number:
Japanese Patent JP2013159685
Kind Code:
A
Abstract:

To efficiently produce a high-quality fatty acid ester, which is usable as a biodiesel fuel, from a free fatty acid residual oil.

A free fatty acid residual oil is esterified by reacting it with a monovalent alcohol in the presence of a cation exchange resin, and a resulting esterification reaction solution is treated with an anion exchange resin. The use of the cation exchange resin as an esterification catalyst allows production of a fatty acid ester at a high conversion rate with an addition amount of the monovalent alcohol substantially equal to a stoichiometric proportion, and a subsequent treatment with the anion exchange resin allows a transesterification reaction of a triglyceride derived from a raw material by the catalytic effect of the anion exchange resin, in addition to adsorptive removal of the residual fatty acid or a pigment component. As a result, the high-purity fatty acid ester can be efficiently produced.


Inventors:
KITAGAWA NAOMI
YONEMOTO TOSHIKUNI
IHARA TORU
TAKAYANAGI HIROAKI
Application Number:
JP2012021989A
Publication Date:
August 19, 2013
Filing Date:
February 03, 2012
Export Citation:
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Assignee:
MITSUBISHI CHEM CORP
TOHOKU TECHNO ARCH CO LTD
International Classes:
C11C3/08; C10L1/02; C10L1/08; C11B3/10; C11C3/10
Domestic Patent References:
JP2010195938A2010-09-09
JP2009190989A2009-08-27
JP2008001856A2008-01-10
JP2010209284A2010-09-24
JP2010195938A2010-09-09
Attorney, Agent or Firm:
Tsuyoshi Shigeno