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Title:
METHOD FOR PRODUCING P-NITROPHENYL SULFATE
Document Type and Number:
Japanese Patent JP2017119648
Kind Code:
A
Abstract:
PROBLEM TO BE SOLVED: To provide a method for producing a p-nitrophenyl sulfate (PNPS salt) such as potassium p-nitrophenyl sulfate (PNPS-K).SOLUTION: A p-nitrophenyl sulfate is produced by reacting p-nitrophenol (PNP) with sulfur trioxide complex in a medium having a low capacity of dissolving p-nitrophenyl sulfate such as tetrahydrofuran, and neutralizing the reaction product with tert-butoxy salt.SELECTED DRAWING: None

Inventors:
MORI KENICHI
Application Number:
JP2015256932A
Publication Date:
July 06, 2017
Filing Date:
December 28, 2015
Export Citation:
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Assignee:
AJINOMOTO KK
International Classes:
C07C303/24; C07C303/44; C07C305/24
Domestic Patent References:
JPS5759853A1982-04-10
JP2014181185A2014-09-29
Foreign References:
DE2830060A11980-01-17
US2402647A1946-06-25
Other References:
MARZEC, KRZYSZTOF ET AL, BULLETIN OF THE POLISH ACADEMY OF SCIENCES, CHEMISTRY, vol. Vo.37, No.9-12, JPN6019038952, 1989, pages 371 - 373, ISSN: 0004131693
Attorney, Agent or Firm:
Sakai International Patent Office