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Title:
METHOD FOR PRODUCING POLYAMIDE
Document Type and Number:
Japanese Patent JP2002212284
Kind Code:
A
Abstract:

To provide a method for producing a polyamide with enhanced production efficiency by adding a diamine to a dicarboxylic acid in the molten state in the absence of a solvent to carry out direct polycondensation.

The method for producing a polyamide conducts the polycondensation of a xylylene diamine with a dicarboxylic acid and comprises, (1) after melting the dicarboxylic acid, (2) a step of adding the amine to the dicarboxylic acid in the molten state in a batchwise first polymerization vessel to obtain a middle stage polymerized product by polycondensation reaction, (3) a step of continuously feeding the middle stage polymerized product to a second polymerization vessel while controlling the change in the relative viscosity of the middle stage polymerized product within ±0.2, and (4) a step of further conducting polycondensation reaction in the continuous second polymerization vessel to obtain a late stage polymerized product.


Inventors:
TANAKA KAZUMI
SHIDA TAKATOSHI
KUROSE HIDEYUKI
Application Number:
JP2001010532A
Publication Date:
July 31, 2002
Filing Date:
January 18, 2001
Export Citation:
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Assignee:
MITSUBISHI GAS CHEMICAL CO
International Classes:
C08G69/30; C08G69/04; C08G69/28; (IPC1-7): C08G69/28
Domestic Patent References:
JPH06145343A1994-05-24
JPS6451433A1989-02-27
JPS58111829A1983-07-04
JPH02245026A1990-09-28
JPH07324130A1995-12-12
JPH0718072A1995-01-20
JPS6474224A1989-03-20
JPH09104751A1997-04-22
Foreign References:
WO1999061511A11999-12-02