Title:
精製ポリテトラフルオロエチレン粉末の製造方法及び低分子量ポリテトラフルオロエチレン粉末
Document Type and Number:
Japanese Patent JP7385150
Kind Code:
B2
Abstract:
The purpose of the present disclosure is to provide a method for producing, from low-molecular-weight polytetrafluoroethylene, refined polytetrafluoroethylene powder in which short-chain fluorine compounds are reduced. The present disclosure is a method for producing refined polytetrafluoroethylene powder from low-molecular-weight polytetrafluoroethylene powder obtained through radical polymerization, the method including a step for reducing short-chain fluorine compounds, where at least compounds represented by general formula (1) are reduced to 179 ppb or less and compounds represented by general formula (2) are reduced to 6900 ppb or less in the abovementioned step. General formula (1): (H-(CF2)m-COO)pM1 (in the formula, m is 3-20, and M1 is H, a metal atom, NR5 4 (where R5 may be the same or different and are H or a C1-10 organic group), imidazolium optionally having a substituent, pyridinium optionally having a substituent, or phosphonium optionally having a substituent. p is 1 or 2.) General formula (2): (H-(CF2)n-SO3)qM2 (in the formula, n is 4-21. M2 is H, a metal atom, NR5 4 (where R5 are the same as above), imidazolium optionally having a substituent, pyridinium optionally having a substituent, or phosphonium optionally having a substituent. q is 1 or 2.)
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Inventors:
Chisei Iguchi
Masao Kubonai
Eiji Masuda
Masayuki Tsuji
Jiro Hiromoto
Masao Kubonai
Eiji Masuda
Masayuki Tsuji
Jiro Hiromoto
Application Number:
JP2022068411A
Publication Date:
November 22, 2023
Filing Date:
April 18, 2022
Export Citation:
Assignee:
Daikin Industries, Ltd.
International Classes:
C08F14/26
Domestic Patent References:
JP2010180364A |
Foreign References:
WO2020213691A1 | ||||
WO2021053531A1 | ||||
WO2019031617A1 |
Attorney, Agent or Firm:
Patent Attorney Firm WisePlus
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