Login| Sign Up| Help| Contact|

Patent Searching and Data


Title:
METHOD FOR PRODUCING TOLUIDINE COMPOUND
Document Type and Number:
Japanese Patent JP2009242370
Kind Code:
A
Abstract:

To provide a production method of fluazinam which is an excellent agrichemical active component and highly useful, by a simple treating operation, at a low cost, with a method being friendly to the environment, efficiently, and in a form of fitting for the purpose.

This production method comprises (1) a process in which ACTF and DCDNBTF are reacted in the presence of an alkali component and a solvent selected from the group consisting of ethers, nitriles, and esters, (2) a process in which the reaction mixture is neutralized or acidified with an acid, and (3) a process in which a crystal of the product is precipitated by distilling off the solvent from the mixture containing the reaction product, that is, fluazinam and the solvent, and it can use an industrially advantageous reaction system and produce the object in an excellent yield.


Inventors:
MURAI SHIGEO
YOSHIZAWA HIROSHI
OSHIMA TAKESHI
MURAKAMI KATSUMI
ANDO TAKAYOSHI
NAKAMURA TADASHI
ADACHI NORIO
ISOGAI AKIHIKO
Application Number:
JP2008178346A
Publication Date:
October 22, 2009
Filing Date:
July 08, 2008
Export Citation:
Click for automatic bibliography generation   Help
Assignee:
ISHIHARA SANGYO KAISHA
International Classes:
C07D213/74
Attorney, Agent or Firm:
Mizuno Akinori