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Title:
METHOD FOR PRODUCING VINYL ACETAL RESIN
Document Type and Number:
Japanese Patent JP2012131923
Kind Code:
A
Abstract:

To provide a method for efficiently producing in a short time a vinyl acetal resin of high acetalization degree in a granular form of excellent handleability.

The method for producing a vinyl acetal resin comprises: a reaction step of obtaining a reaction liquid with a vinyl acetal resin dispersed highly therein by subjecting a mixed liquid of an aldehyde and a vinyl alcohol-based resin or vinyl acetate-based resin solution to an acetalization reaction in a high-temperature and high-pressure fluid of 100-400°C and 0.5-100 MPa; and a granulation step of obtaining the objective granular vinyl acetal resin by charging the reaction liquid, via small holes, into water at a temperature lower than the glass transition temperature of the vinyl acetal resin obtained by the preceding step.


Inventors:
NISHIMURA YOHEI
NAGAI YASUHARU
Application Number:
JP2010286028A
Publication Date:
July 12, 2012
Filing Date:
December 22, 2010
Export Citation:
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Assignee:
SEKISUI CHEMICAL CO LTD
International Classes:
C08J3/12; C08F8/28; C08F18/08
Domestic Patent References:
JP2006089536A2006-04-06
JP2004143405A2004-05-20
JP2005060535A2005-03-10
JPH04258638A1992-09-14
JPWO2008096403A12010-05-20
JP2010106234A2010-05-13
JPWO2005073285A12007-09-13
JP2007502723A2007-02-15
Foreign References:
WO2008096403A12008-08-14
WO2005073285A12005-08-11
Attorney, Agent or Firm:
Atomi International Patent Office