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Title:
METHOD FOR PURIFYING (-)-N-ISOPULEGOL AND CITROUS PREFUME COMPOSITION, OBTAINED BY THE SAME METHOD AND CONTAINING (-)-N-ISOPULEGOL
Document Type and Number:
Japanese Patent JP3241542
Kind Code:
B2
Abstract:

PURPOSE: To purify isopulegol to the subject chemically and optically high-purity compound, capable of imparting the refreshingness, freshness and a cool feeling to an aroma of the perfume composition and excellent in odorless properties by carrying out the subzero treatment of the isopulegol with a specific subzero treating solvent.
CONSTITUTION: This method for purifying isopulegol is to carry out the subzero treatment of (A) the isopulegol consisting essentially of the (-)-n-isomer with (B) a subzero treating solvent consisting essentially of acetone and purify the component (A) to (-)-n-isopulegol of ≥99.7% chemical purity and ≥99.7% optical purity. Furthermore, the (-)-n-isopulegol obtained by the purification is preferably used as a component of a citrous perfume composition and the amount thereof used is 3-30wt.% based on the citrous perfume composition.


Inventors:
Ken Yamamoto
Application Number:
JP19628294A
Publication Date:
December 25, 2001
Filing Date:
July 29, 1994
Export Citation:
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Assignee:
Takasago International Corporation
International Classes:
A61Q13/00; C07C29/78; C07C29/80; C07C35/17; C07C35/18; A61K8/00; C11B9/00; C11B9/02; (IPC1-7): C07C35/17; A61K7/46; C07C29/78; C11B9/00; C11B9/02
Domestic Patent References:
JP665023A
JP53116348A
Attorney, Agent or Firm:
Kazuo Watanabe