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Title:
染着ポリエステル繊維からの有効成分回収方法
Document Type and Number:
Japanese Patent JP4537288
Kind Code:
B2
Abstract:

To establish a method for efficiently and economically recovering high-purity useful component(s) from dyed polyester textile products.

The method for recovering useful component(s) from dyed polyester (PES) fiber comprises a dye extraction step, a solid/liquid separation step, a depolymerization step, a transesterification step and a useful component recovering step. Specifically, the method comprises the following process: The dye extraction step is conducted at a temperature higher than the glass transition temperature of the PES but at 220°C or lower using an extractive solvent consisting of a xylene and an alkylene glycol. In the solid/liquid separation step, the dye-extracted PES fiber and the resultant dye-containing extractive solvent are separated from each other. In the depolymerization step, the dye-extracted PES fiber is depolymerized while additionally charging part of a depolymerization reaction liquid to the system to obtain a depolymerization solution. In the transesterification step, methanol is added to the depolymerization solution to conduct a transesterification. In the useful component recovering step, dimethyl terephthalate and the alkylene glycol are separated and recovered from the resulting transesterification product mixture.

COPYRIGHT: (C)2007,JPO&INPIT


Inventors:
Koji Mukai
Minoru Nakajima
Application Number:
JP2005229291A
Publication Date:
September 01, 2010
Filing Date:
August 08, 2005
Export Citation:
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Assignee:
TEIJIN FIBERS LIMITED
International Classes:
C08J11/24; B01D3/14; B01D11/02; C07C31/20; C07C67/03; C07C69/82; C08J11/08; C07B61/00; C08L67/00
Domestic Patent References:
JP2003128626A
JP2004300115A
JP2004217871A
JP2002167357A
JP2002167341A
Foreign References:
WO2001019775A1
Attorney, Agent or Firm:
Hideko Mihara



 
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