To provide a multi-stage method for continuously producing an alicyclic diisocyanate without containing phosgene.
This multi-stage method for continuously producing the alicyclic diisocyanate comprises synthesizing an alicyclic diurethane by reacting an alicyclic diamine and an alcohol with urea and/or a urea derivative, removing easily-boiling substances and intermediately-boiling substances from the diurethane, thermally decomposing the diurethane so as to isolate the desired diisocyanate, continuously discharging a part of a bottom reaction product of a decomposing column from a decomposing apparatus, separating a high-boiling component from the discharged product, re-urethanating the discharged product by using the alcohol, and recirculating the re-urethanated product in the above processes.
KRECZINSKI MANFRED
ELM RAINER DR
MICHALCZAK HANS-WERNER
JPH0625136A | 1994-02-01 | |||
JPH02101057A | 1990-04-12 | |||
JPH0625136A | 1994-02-01 | |||
JPH02101057A | 1990-04-12 |
Toshiomi Yamazaki
Takuya Kuno
Einzel Felix-Reinhard
Reinhard Einsel