Title:
PREPARATION OF 4,6-DIAMINORESORCIN AND ITS SALT
Document Type and Number:
Japanese Patent JPH116090
Kind Code:
A
Abstract:
To prepare 4,6-diaminoresorcin and its salt as stock monomers of polybenzobisoxazole by electrolytically reducing 4,6-bis-substd. phenylazoresorcinol.
4,6-Bis-substd. phenylazoresorcinol represented by the formula [where R1 and R2 are individually H, 1-10C alkyl, 1-10C alkoxy, halogen, sulfonic acid, cyano, carboxyl or 2-11C carboalkoxy and (n) and (m) are integers of 0-5] is electrolytically reduced in an acidic solvent or its aq. soln. such as an aq. hydrochloric acid soln. or a mixed solvent consisting of an acidic solvent or its aq. soln. and an org. solvent such as dioxide or ethanol.
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Inventors:
NISHIGUCHI IKUZO
MAEKAWA HIROSHI
SUZUKI HIDEO
AKIMOTO KAZUHIKO
MAEKAWA HIROSHI
SUZUKI HIDEO
AKIMOTO KAZUHIKO
Application Number:
JP16080997A
Publication Date:
January 12, 1999
Filing Date:
June 18, 1997
Export Citation:
Assignee:
NISSAN CHEMICAL IND LTD
International Classes:
C25B3/25; (IPC1-7): C25B3/04
Next Patent: JPH0116091