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Title:
PREPARATION OF LIGHT-COLORED ISOCYANATE
Document Type and Number:
Japanese Patent JP2009149614
Kind Code:
A
Abstract:

To provide a light-colored isocyanate as a raw material for a light-colored or uncolored polyisocyanate.

The method for producing the light-colored isocyanate is regulated as follows. The PRI (polarographically reducible impurity) value of a start amine is regulated so as to be 60 mpm (mol per million mol) in a reaction of the amine with phosgene in vapor phase. The reaction in a reaction zone is carried out at a temperature of 200C and 570C under an absolute pressure of 0.8-3 bar. The pressure in an amine- or phosgene-feeding line is regulated so as to be 20-2,000 mbar higher than the pressure in the reaction zone, and the pressure in a downstream zone of the reaction zone is regulated so as to be 10-500 mbar lower than the pressure in the reaction zone.


Inventors:
Stutz, Herbert
Halpaap, Dr. Reinhard
Lewkebandara, Tilak Suren
Application Number:
JP2008000291120
Publication Date:
July 09, 2009
Filing Date:
November 13, 2008
Export Citation:
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Assignee:
BAYER MATERIALSCIENCE AG
BAYER MATERIAL SCIENCE LLC
International Classes:
C07C263/10; C07C265/14