To provide a light-colored isocyanate as a raw material for a light-colored or uncolored polyisocyanate.
The method for producing the light-colored isocyanate is regulated as follows. The PRI (polarographically reducible impurity) value of a start amine is regulated so as to be 60 mpm (mol per million mol) in a reaction of the amine with phosgene in vapor phase. The reaction in a reaction zone is carried out at a temperature of 200C and 570C under an absolute pressure of 0.8-3 bar. The pressure in an amine- or phosgene-feeding line is regulated so as to be 20-2,000 mbar higher than the pressure in the reaction zone, and the pressure in a downstream zone of the reaction zone is regulated so as to be 10-500 mbar lower than the pressure in the reaction zone.
|JP05320297||PREPARATION OF POLYAMINE FOR LIGHTER COLOR POLYISOCYANATE BASED FOAM|
|WO/2006/048171||METHOD FOR PRODUCING POLYISOCYANATES|
|WO/2007/014936||METHOD FOR PRODUCING DIISOCYANATES|
Halpaap, Dr. Reinhard
Lewkebandara, Tilak Suren
BAYER MATERIAL SCIENCE LLC