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Title:
PREPARATION OF LIGHT-COLORED ISOCYANATE
Document Type and Number:
Japanese Patent JP2009149614
Kind Code:
A
Abstract:

To provide a light-colored isocyanate as a raw material for a light-colored or uncolored polyisocyanate.

The method for producing the light-colored isocyanate is regulated as follows. The PRI (polarographically reducible impurity) value of a start amine is regulated so as to be 60 mpm (mol per million mol) in a reaction of the amine with phosgene in vapor phase. The reaction in a reaction zone is carried out at a temperature of 200C and 570C under an absolute pressure of 0.8-3 bar. The pressure in an amine- or phosgene-feeding line is regulated so as to be 20-2,000 mbar higher than the pressure in the reaction zone, and the pressure in a downstream zone of the reaction zone is regulated so as to be 10-500 mbar lower than the pressure in the reaction zone.


Inventors:
STUTZ HERBERT
HALPAAP REINHARD DR
LEWKEBANDARA TILAK SUREN
Application Number:
JP2008291120A
Publication Date:
July 09, 2009
Filing Date:
November 13, 2008
Export Citation:
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Assignee:
BAYER MATERIALSCIENCE AG
BAYER MATERIALSCIENCE LLC
International Classes:
C07C263/10; C07C265/14
Domestic Patent References:
JPH0687815A1994-03-29
JPH11240858A1999-09-07
JP2007326857A2007-12-20
JPH0687815A1994-03-29
JPH11240858A1999-09-07
JP2008503532A2008-02-07
JPH05320297A1993-12-03
JP2003503383A2003-01-28
JP2008545745A2008-12-18
JP2004513105A2004-04-30
JP2006510692A2006-03-30
Foreign References:
US20070232827A12007-10-04
Attorney, Agent or Firm:
Mitsuo Tanaka
Takuji Yamada
Kenichi Morizumi
Yasuo Shibata
Yasushi Ochiai