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Title:
PREPARATION OF TRUELY SPHERICAL POWDER OF SAPONIFIED ETHYLENE-VINYL ACETATE COPOLYMER OR THE SAME MODIFIED BY CARBOXYL GROUP
Document Type and Number:
Japanese Patent JPS56145925
Kind Code:
A
Abstract:

PURPOSE: To obtain truely spherical powder, having a uniform particle diameter, by mixing a saponified ethylene-vinyl acetate copolymer with an adduct of alkylphenol and ethylene oxide and stirring to emulsify the mixture.

CONSTITUTION: 100pts.wt. Saponified ethylene-vinyl acetate copolymer having a content of vinyl acetate group of 5W50wt% or the same modified by carboxyl groups which is obtained by reacting the same with an unsaturated carboxylic acid or cyclic carboxylic anhydride is mixed with 10W100pts.wt. organic solvent with a boiling point of 80°C or higher which dissolves the above-mentioned saponified copolymer or the same modified by carboxyl groups and is not freely miscible with water, 300W1,000pts.wt. water, and 0.1W10pts.wt. adduct of alkylphenol and ethylene oxide having a HLB value of 10W20. Then the mixture is emulsified maintaining its temperature above the softening point of the above-mentioned saponified copolymer or the same modified by carboxyl groups, and thereafter, the temperature of the system is, under stirring, lowered below the above-mentioned softening point.


Inventors:
NAKABAYASHI MASAMITSU
DOUURA FUMIHIRO
FURUKAWA YUUZOU
Application Number:
JP4995780A
Publication Date:
November 13, 1981
Filing Date:
April 15, 1980
Export Citation:
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Assignee:
TAKEDA CHEMICAL INDUSTRIES LTD
International Classes:
C08F8/00; C08F8/46; C08F255/00; C08F255/02; C08F289/00; C08J3/12; C09D5/00; C09D5/03; C09D129/04; (IPC1-7): C08F8/46; C08F255/02; C08J3/12; C09D3/74; C09D5/00