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Title:
PROCESS FOR PRODUCING CARBOXYMETHYL CELLULOSE SALT
Document Type and Number:
Japanese Patent JP2006241374
Kind Code:
A
Abstract:

To provide a carboxymethyl cellulose salt (CMC salt) that suppresses the reduction in its viscosity to the utmost and has an enhanced powder whiteness.

A method for producing the above CMC salt comprises a step (a) of producing an aqueous solution of the CMC salt by converting a cellulose to an alkali cellulose and etherifying the alkali cellulose, a step (b) of separating the CMC salt by neutralizing the aqueous solution of the CMC salt and a step (c) of bleaching the CMC salt with a bleaching agent, wherein the aqueous solution of the CMC salt after neutralized in the step (b) has a pH of 7.0-9.0; the weight ratio of a solvent to a CMC salt solid matter in the CMC salt separated from the aqueous solution of the CMC salt is 0.5-3.0; and in the step (c), a 1-5 wt% aqueous solution of hydrogen peroxide as a bleaching agent is added at 40-80°C in an amount of 2-10 pts.wt. based on 100 pts.wt. CMC salt.


Inventors:
SATO KEIICHI
Application Number:
JP2005061320A
Publication Date:
September 14, 2006
Filing Date:
March 04, 2005
Export Citation:
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Assignee:
DAI ICHI KOGYO SEIYAKU CO LTD
International Classes:
C08B11/12
Domestic Patent References:
JPH0425501A1992-01-29
JPH0425502A1992-01-29
JP2000119303A2000-04-25
JP2000290301A2000-10-17
JPH09309972A1997-12-02
JPS6031501A1985-02-18
JPS6253301A1987-03-09
JPS4819232B11973-06-12
JPS45678B1
JPH0425501A1992-01-29
JPH0425502A1992-01-29
JP2000119303A2000-04-25
JP2000290301A2000-10-17
JPH09309972A1997-12-02
JPS6031501A1985-02-18
JPS6253301A1987-03-09
JPS4819232B11973-06-12
JPS45678B1
Foreign References:
US2912431A1959-11-10
US3394127A1968-07-23
US2912431A1959-11-10
US3394127A1968-07-23
Attorney, Agent or Firm:
Sota Asahina
Fumio Akiyama