Title:
PRODUCTION OF 1-HEXENE
Document Type and Number:
Japanese Patent JP3890628
Kind Code:
B2
Abstract:
PROBLEM TO BE SOLVED: To produce 1-hexene without separating the by-product from the system or causing the clogging of the apparatus by trimerizing ethylene in the presence of a chromium-based catalyst, deactivating the catalyst, introducing water into the treating system and stirring the mixture to effect the deashing treatment.
SOLUTION: Ethylene is trimerized in the presence of a chromium-based catalyst composed of a chromium compound and an alkyl metal compound and the chromium-based catalyst is deactivated after completing the trimerization reaction. Water is introduced in an amount of 20-200vol.% based on the liquid reaction product into the treating system while keeping the liquid reaction product at 100-180°C and the system is stirred with a stirring power of ≥1KW/m3 to effect the deashing treatment by the removal of the metallic component originated from the chromium-based catalyst from the liquid reaction product and obtain 1-hexene useful as a comonomer of a linear low-density polyethylene or a raw material for plasticizers.
Inventors:
Motohiro Oguri
Takamitsu Aoyama
Toshihide Yamamoto
Hideyuki Mimura
Yasuyuki Koie
Takamitsu Aoyama
Toshihide Yamamoto
Hideyuki Mimura
Yasuyuki Koie
Application Number:
JP15580596A
Publication Date:
March 07, 2007
Filing Date:
June 17, 1996
Export Citation:
Assignee:
Tosoh Corporation
International Classes:
B01J31/12; C07C11/107; B01J31/14; B01J31/22; C07B61/00; C07C2/30; C07C2/32; C07C7/148; (IPC1-7): C07C11/107; B01J31/12; B01J31/14; B01J31/22; C07C2/30; C07C2/32; C07C7/148; //C07B61/00
Domestic Patent References:
| JP7149674A | ||||
| JP3220135A | ||||
| JP8053374A | ||||
| JP7242701A | ||||
| JP63041430A |
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