Title:
PRODUCTION OF 2,2,6,6-TETRAMETHYL-4-HYDROXYPIPERIDINE
Document Type and Number:
Japanese Patent JPH09316054
Kind Code:
A
Abstract:
To provide a method for producing the subject compound by catalytic hydrogenation of 2,2,6,6-tetramethyl-4-piperidone and enabling circulating reuse of the hydrocarbon solvent used in the reaction without affecting the quality of the final product at all.
In the method for producing 2,2,6,6-tetramethyl-4- hydroxypiperidine by hydrogenating 2,2,6,6-tetramethyl-4-piperidone in the presence of a hydrogenation catalyst in a hydrocarbon solvent, the mother liquid after recovering the 2,2,6,6-tetramethyl-4-hydroxypiperidine crystallized from the reaction mixture after the reaction is treated with an acid and then circulated and reused as a solvent for the reaction.
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Inventors:
INUI YUKIYOSHI
AOYAMA KATSUNORI
AOYAMA KATSUNORI
Application Number:
JP12994296A
Publication Date:
December 09, 1997
Filing Date:
May 24, 1996
Export Citation:
Assignee:
MITSUBISHI CHEM CORP
International Classes:
C07D211/46; B01J25/02; C07B61/00; (IPC1-7): C07D211/46; B01J25/02
Attorney, Agent or Firm:
長谷川 曉司
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