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Patent Searching and Data


Title:
PRODUCTION OF POLYBENZAZOLE FIBER
Document Type and Number:
Japanese Patent JPH0860436
Kind Code:
A
Abstract:

PURPOSE: To obtain a polybenzazole fiber hardly having denier unevenness in the longitudinal direction, excellent in uniformity and having high strength and modulus by subjecting polybenzazole dope to dry wet spinning through a specific spinneret.

CONSTITUTION: A polybenzazole polymer solution polymerized in a polyphosphoric acid solvent is directly used as a spinning dope and kneaded and subjected to defoaming treatment in a two-axle kneader and fed to a spinning head and spinning fine holes radially extended from the center of a spinneret are divided and perforated by a dividing zone 3 which is not perforated and discharged through spinneret having ≥2.0/cm2 and <5.0/cm2 hole density of a spinning hole group 2 to form dope filaments to form dope filament and successively actively cooled in stream kept to 30-100°C in an air gap and brought into contact with a solvent-insoluble coagulating bath of a phosphoric acid water solution and taken off to provide the objective polybenzazole fiber having relatively fine single yarn at high spinning rate of ≥200m/min in good productivity.


Inventors:
TANI KATSUYA
IBA IHACHIRO
Application Number:
JP19063594A
Publication Date:
March 05, 1996
Filing Date:
August 12, 1994
Export Citation:
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Assignee:
TOYO BOSEKI
International Classes:
C08G75/32; C08G73/18; C08G73/22; C08G75/00; D01D4/02; D01D5/06; D01D5/26; D01F6/74; (IPC1-7): D01F6/74; C08G73/18; C08G73/22; C08G75/32; D01D5/06