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Title:
PRODUCTION OF PRECURSOR PITCH FOR CARBON FIBER
Document Type and Number:
Japanese Patent JPS61162586
Kind Code:
A
Abstract:

PURPOSE: To obtain the titled pitch of low viscosity with good thermal stability and spinnability without hydrogenation-treatment, etc., by removing the high- molecular weight component in tar pitch by solvent extraction followed by heat-treatment of the resultant pitch.

CONSTITUTION: First, tar pitch is subjected to extraction-treatment with an aromatic solvent (e.g., tar-based middle oil) followed by separation-treatment such as filtration to eliminate solvent-insolubles. Next, the resulting pitch is treated by heating (pref. being heated to 470W530°C under an inert gas atmo sphere and a reduced pressure ≤20mmHg at a rate ≥15°C/min. followed by heating at this highest temperature for ≤10min), thus obtaining the objective pitch. The elimination of solvent-insolubles mentioned above is pref. carried out in such a manner that the pyridine-insolubles and quinoline-insolubles in the pitch represent ≤2wt% and trace amount, respectively.


Inventors:
OOSUGI YUKIHIRO
YUMITATE KOZO
KAMISHITA MAMORU
Application Number:
JP39385A
Publication Date:
July 23, 1986
Filing Date:
January 08, 1985
Export Citation:
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Assignee:
KAWASAKI STEEL CO
NITTO BOSEKI CO LTD
International Classes:
C10C3/08; C10C3/02; C10C3/04; C10C3/10; D01F9/14; D01F9/15; (IPC1-7): C10C3/08; D01F9/14
Domestic Patent References:
JPS5938280A1984-03-02
JPS5947426A1984-03-17
JPS57141487A1982-09-01
JPS58156025A1983-09-16
JPS60170694A1985-09-04
Attorney, Agent or Firm:
Akihide Sugimura