PURPOSE: To obtain the titled pitch of low viscosity with good thermal stability and spinnability without hydrogenation-treatment, etc., by removing the high- molecular weight component in tar pitch by solvent extraction followed by heat-treatment of the resultant pitch.
CONSTITUTION: First, tar pitch is subjected to extraction-treatment with an aromatic solvent (e.g., tar-based middle oil) followed by separation-treatment such as filtration to eliminate solvent-insolubles. Next, the resulting pitch is treated by heating (pref. being heated to 470W530°C under an inert gas atmo sphere and a reduced pressure ≤20mmHg at a rate ≥15°C/min. followed by heating at this highest temperature for ≤10min), thus obtaining the objective pitch. The elimination of solvent-insolubles mentioned above is pref. carried out in such a manner that the pyridine-insolubles and quinoline-insolubles in the pitch represent ≤2wt% and trace amount, respectively.
YUMITATE KOZO
KAMISHITA MAMORU
NITTO BOSEKI CO LTD
JPS5938280A | 1984-03-02 | |||
JPS5947426A | 1984-03-17 | |||
JPS57141487A | 1982-09-01 | |||
JPS58156025A | 1983-09-16 | |||
JPS60170694A | 1985-09-04 |
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