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Title:
REGENERATION AND USE OF LACTIC ACID-BASED BY-PRODUCT
Document Type and Number:
Japanese Patent JPH10182630
Kind Code:
A
Abstract:

To provide a process for producing lactic acid by regenerating a by-product produced in a production process of a lactic acid-based composition and, at the same time, producing a lactide and a polylactic acid having arbitrary optical purity using the regenerated lactic acid.

An essentially optically inactive lactic acid component is produced from a lactic acid component in a condensed water, a still residue, process washing liquid, vacuum pump waste liquid in a direct synthesis of a lactic acid prepolymer or a polylactic acid, still residue, process washing liquid, waste liquid discharged from a vacuum pump, etc., in a depolymerziation of the lactic acid prepolymer to obtain lactide, a waste liquid of a lactide purification process such as process washing liquid and a vacuum pump waste liquid, a loss generated in the molding of a polylactic acid such as a waste polymer produced in the polymerization of a lactide to form a polylactic acid, a waste polymer generated in the market, etc., by racemizing the above raw materials in the presence or absence of a catalyst. An optically inactive lactide or polylactic acid is produced from the optically inactive lactic acid component and the produced lactide or polylactic acid is mixed with a lactide or a polylactic acid having an optical purity of 90-100%e.e. at an arbitrary ratio to obtain a lactide or polylactic acid having arbitrary optical purity.


Inventors:
OKUYAMA HISATSUGU
OGUCHI MAKOTO
KAWAMOTO TATSUJI
KAWABE TAKASHI
HORIBE YASUMASA
Application Number:
JP34571796A
Publication Date:
July 07, 1998
Filing Date:
December 25, 1996
Export Citation:
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Assignee:
SHIMADZU CORP
International Classes:
B01J31/04; C07B55/00; C07B61/00; C07C67/465; C07C69/708; C08G63/06; C08G63/08; C08J11/00; C08J11/10; C07D319/12; (IPC1-7): C07D319/12; B01J31/04; C08G63/06; C08G63/08; C08J11/00; C08J11/10
Attorney, Agent or Firm:
Yoshiaki Nishioka