Title:
A manufacturing method of the Poriro taxane which has a block machine
Document Type and Number:
Japanese Patent JP6013459
Kind Code:
B2
Abstract:
The invention provides a method of producing a polyrotaxane having cyclic molecules, a linear molecule threaded through the cyclic molecules to form a clathrate, and blocking groups at both ends of the linear molecule to prevent the separation of the cyclic molecules from the linear molecule, the method including forming the blocking groups by reacting the linear molecule piercing the cyclic molecules, the linear molecule having carboxyl groups at both ends thereof, with a blocking agent having an amino group in the absence of a solvent or in at least one organic solvent selected from the group consisting of aprotic amide solvents and aromatic hydrocarbons, and further in the presence of 2.0 mol to 100 mol of a triazine-based amidating agent per 1 mol of the carboxyl groups in the linear molecule.
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Inventors:
Naoyuki Yokota
Kenji Arimitsu
Akio Matsushita
Takashi Okami
Mikio Fujimoto
Yasunori Fukuda
Minoru Iwata
Yuuki Hayashi
Kenji Arimitsu
Akio Matsushita
Takashi Okami
Mikio Fujimoto
Yasunori Fukuda
Minoru Iwata
Yuuki Hayashi
Application Number:
JP2014508255A
Publication Date:
October 25, 2016
Filing Date:
April 01, 2013
Export Citation:
Assignee:
Ube Industries,Ltd.
Advanced Soft Materials Co., Ltd.
Advanced Soft Materials Co., Ltd.
International Classes:
C08G65/333; C08B37/16
Domestic Patent References:
| JP2005154675A | ||||
| JP2010174105A |
Foreign References:
| WO2005095493A1 | ||||
| WO2005080469A1 | ||||
| WO2009041666A1 |
Other References:
Dawson R.E. et. al,Synthesis of α-cyclodextrin [2]-rotaxanes using chlorotriazine capping reagents,Organic and Biomolecular Chemistry,2008年,vol.6,p.1814-1821
Attorney, Agent or Firm:
Patent business corporation Tsukuni
Hajime Tsukuni
Toshio Miyake
Akio Shibata
Hajime Tsukuni
Toshio Miyake
Akio Shibata
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