Title:
フラノース誘導体の製造方法
Document Type and Number:
Japanese Patent JP5550234
Kind Code:
B2
Abstract:
An object of the present invention is to provide a industrially appropriate method for producing the ²-anomers of ribofuranose derivatives in a highly selective manner at a high yield. The present invention provides a method for producing ribofuranose derivatives wherein ²-anomers is precipitated from among the generated furanose derivatives by controlling the amount of a reaction reagent used and/or using a poor solvent in the acetolysis reactions of 2,3,5-tri-O-acyl-1-O-alkyl-ribofuranose and 2,3-di-O-acyl-1-O-alkyl-5-deoxy-ribofuranose.
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Inventors:
Manabu Katsurada
Tomoko Sasaki
Yasuko Nakajima
Nobuo Omura
Tomoko Sasaki
Yasuko Nakajima
Nobuo Omura
Application Number:
JP2008548347A
Publication Date:
July 16, 2014
Filing Date:
December 07, 2007
Export Citation:
Assignee:
API, Inc. Corporation
International Classes:
C07H1/06; C07H13/06
Domestic Patent References:
| JP2002503212A | 2002-01-29 | |||
| JP2005539032A | 2005-12-22 |
Other References:
JPN6013026291; Ｔｅｔｒａｈｅｄｒｏｎ Ｌｅｔｔｅｒｓ Ｖｏｌ． ４２, 2001, ７６５１-７６５３
JPN6013026293; Ｊｏｕｒｎａｌ ｏｆ Ｍｅｄｉｃｉｎａｌ Ｃｈｅｍｉｓｔｒｙ Ｖｏｌ． ４３， Ｎｏ． １３, 2000, ２５６６-２５７４
JPN6013026294; Ｊｏｕｒｎａｌ ｏｆ Ｍｅｄｉｃｉｎａｌ Ｃｈｅｍｉｓｔｒｙ Ｖｏｌ． ４３， Ｎｏ． ５, 2000, １０１９-１０２８
JPN6013026296; Ｈｅｌｖｅｔｉｃａ Ｃｈｉｍｉｃａ Ａｃｔａ Ｎｏ． １２１, 1959, １１７１-１１７３
JPN6008010647; ＧＵＴＨＲＩＥ， Ｒ． Ｄ． ｅｔ ａｌ．: 'Ａｎ ｉｍｐｒｏｖｅｄ ｐｒｅｐａｒａｔｉｏｎ ｏｆ １，２，３，５-ｔｅｔｒａ-Ｏ-ａｃｅｔｙｌ-beta-Ｄ-ｒｉｂｏｆｕｒａｎｏｓｅ' Ｃｈｅｍｉｓｔｒｙ ＆ Ｉｎｄｕｓｔｒｙ Ｎｏ．１７, 1968, ｐｐ．５４７-５４８
JPN6013026297; Ｏｒｇａｎｉｃ Ｐｒｏｃｅｓｓ Ｒｅｓｅａｒｃｈ ＆ Ｄｅｖｅｌｏｐｍｅｎｔ Ｖｏｌ． ９， Ｎｏ． ５, 2005, ５８３-５９２
JPN6013026299; Ｃａｒｂｏｈｙｄｒａｔｅ Ｒｅｓｅａｒｃｈ Ｖｏｌ． ３３８, 2003, ３０３-３０６
JPN6014017816; Ｊｏｕｒｎａｌ ｏｆ Ｃａｒｂｏｈｙｄｒａｔｅ Ｃｈｅｍｉｓｔｒｙ １３（８）, 1994, １１１５-１１１９
JPN6013026293; Ｊｏｕｒｎａｌ ｏｆ Ｍｅｄｉｃｉｎａｌ Ｃｈｅｍｉｓｔｒｙ Ｖｏｌ． ４３， Ｎｏ． １３, 2000, ２５６６-２５７４
JPN6013026294; Ｊｏｕｒｎａｌ ｏｆ Ｍｅｄｉｃｉｎａｌ Ｃｈｅｍｉｓｔｒｙ Ｖｏｌ． ４３， Ｎｏ． ５, 2000, １０１９-１０２８
JPN6013026296; Ｈｅｌｖｅｔｉｃａ Ｃｈｉｍｉｃａ Ａｃｔａ Ｎｏ． １２１, 1959, １１７１-１１７３
JPN6008010647; ＧＵＴＨＲＩＥ， Ｒ． Ｄ． ｅｔ ａｌ．: 'Ａｎ ｉｍｐｒｏｖｅｄ ｐｒｅｐａｒａｔｉｏｎ ｏｆ １，２，３，５-ｔｅｔｒａ-Ｏ-ａｃｅｔｙｌ-beta-Ｄ-ｒｉｂｏｆｕｒａｎｏｓｅ' Ｃｈｅｍｉｓｔｒｙ ＆ Ｉｎｄｕｓｔｒｙ Ｎｏ．１７, 1968, ｐｐ．５４７-５４８
JPN6013026297; Ｏｒｇａｎｉｃ Ｐｒｏｃｅｓｓ Ｒｅｓｅａｒｃｈ ＆ Ｄｅｖｅｌｏｐｍｅｎｔ Ｖｏｌ． ９， Ｎｏ． ５, 2005, ５８３-５９２
JPN6013026299; Ｃａｒｂｏｈｙｄｒａｔｅ Ｒｅｓｅａｒｃｈ Ｖｏｌ． ３３８, 2003, ３０３-３０６
JPN6014017816; Ｊｏｕｒｎａｌ ｏｆ Ｃａｒｂｏｈｙｄｒａｔｅ Ｃｈｅｍｉｓｔｒｙ １３（８）, 1994, １１１５-１１１９
Attorney, Agent or Firm:
Patent business corporation patent firm Sykes
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