Title:
低温マイクロ波支援有機化学合成のための方法及び器具
Document Type and Number:
Japanese Patent JP5342097
Kind Code:
B2
Abstract:
An instrument (10) and associated method are disclosed for performing microwave assisted organic chemical synthesis at low temperatures. The instrument (10) includes a reaction vessel (20) formed of a microwave transparent material that defmes an interior reaction chamber (17) for carrying out microwave assisted reactions in the chamber, a cooling jacket (22) immediately surrounding the reaction vessel for cooling the vessel and the vessel (20) contents during the application of microwave energy (25) to contents in the vessel when a microwave transparent media used as a fluid coolant is present in the jacket. The instrument includes means (18) for supplying a microwave transparent fluid coolant to the cooling jacket and means (19) for venting the fluid coolant from the cooling jacket (22), a fluid coolant reservoir (59) in communication with the cooling jacket, and a pump (61) in communication with the reservoir (59) and the cooling jacket (22) for circulating fluid coolant from the fluid coolant reservoir through the cooling jacket and around the reaction vessel.
Inventors:
E Keller Burnhart
Wyatt P. Harget, Jr.
James Edward Thomas
Wyatt P. Harget, Jr.
James Edward Thomas
Application Number:
JP2005238239A
Publication Date:
November 13, 2013
Filing Date:
August 19, 2005
Export Citation:
Assignee:
CM Corporation
International Classes:
B01J19/12; F27D11/12
Foreign References:
| US5345066 | ||||
| WO2004002617A1 |
Attorney, Agent or Firm:
Shinjiro Ono
Kazuo Shamoto
Tadashi Masui
Yasushi Kobayashi
Akio Chiba
Hiroyuki Tomita
Kazuo Shamoto
Tadashi Masui
Yasushi Kobayashi
Akio Chiba
Hiroyuki Tomita