A method of manufacturing a carbonyl compound using the catalyst containing nitroglycerine Hexyl radical in which continuation operation is possible

Title:

A method of manufacturing a carbonyl compound using the catalyst containing nitroglycerine Hexyl radical in which continuation operation is possible

Document Type and Number:

Japanese Patent JP6021892

Kind Code:

B2

Abstract:

The invention relates to a method for the oxidation of a primary or secondary alcohol, preferably to form an aldehyde or ketone, comprising the following steps: a) providing a catalyst composition comprising at least one compound containing a nitroxyl radical, at least one NO source, at least one carbon or mineral acid or an anhydride of a carbon or mineral acid; b) producing a reaction mixture by adding at least one primary or secondary alcohol and a gas comprising oxygen and optionally one or more than one solvent to the catalyst composition from step a) or step e); c) incubating the reaction mixture from step b) at a temperature of between 0 and 100° C. or at the boiling point of the solvent; d) simultaneously with or subsequent to step c): crystallizing the reaction product; and e) recovering the catalyst composition by removing the crystallized reaction product from the reaction mixture obtained in step d).

Inventors:

Florian Klasowski
Thomas hearts
Thomas Tacke
Yan Christoph Pfeffer
Michael linbach
Michael forant
Miheel Janssen
Roger Sheldon
Jürgen Harborland

Application Number:

JP2014504182A

Publication Date:

November 09, 2016

Filing Date:

December 06, 2011

Export Citation:

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