Title:
SINGLE CRYSTAL OF POROUS COMPOUND, QUALITY DISCRIMINATION METHOD OF SINGLE CRYSTAL, PREPARATION METHOD OF SOLUTION INCLUDING COMPOUND TO BE ANALYZED, FABRICATION METHOD OF SAMPLE FOR CRYSTAL STRUCTURE ANALYSIS, AND MOLECULAR STRUCTURE DETERMINATION METHOD OF COMPOUND TO BE ANALYZED
Document Type and Number:
Japanese Patent JP2016166162
Kind Code:
A
Abstract:
PROBLEM TO BE SOLVED: To provide a single crystal suited for a crystal sponge method, a quality discrimination method of the single crystal used for the crystal sponge method, a fabrication method of a sample for crystal structure analysis using the single crystal of which the quality is discriminated by the method, a preparation method of a solution including a compound to be analyzed used for the crystal sponge method, and a fabrication method of the sample for crystal structure analysis using the solution including the compound to be analyzed obtained by the method, as well as a molecular structure determination method of the compound to be analyzed using the sample for crystal structure analysis obtained by the method.SOLUTION: There is provided a single crystal of a porous compound or the like, which is a single crystal used for fabricating a sample for crystal structure analysis of a compound to be analyzed by bringing the single crystal of the porous compound having a three-dimensional skeleton and three-dimensionally and regularly arranged pores and/or hollows formed by partitioning with the three-dimensional skeleton into contact with a solution including the compound to be analyzed and arranging molecules of the compound to be analyzed regularly in the pores and/or hollows, in which an edge of the single crystal is 10-2,000 μm and the single crystal retains single crystallinity even after the single crystal has been brought into contact with a solvent chemically identical to the solvent of the solution including the compound to be analyzed.SELECTED DRAWING: None
Inventors:
FUJITA MAKOTO
INOKUMA YASUHIDE
DOMOTO YUYA
INOKUMA YASUHIDE
DOMOTO YUYA
Application Number:
JP2015047731A
Publication Date:
September 15, 2016
Filing Date:
March 10, 2015
Export Citation:
Assignee:
UNIV TOKYO
International Classes:
C07D401/14
Attorney, Agent or Firm:
Haruhito Oishi
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