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Title:
A recycling method of the ionic liquid used for the manufacturing method of cyclic ether, and it
Document Type and Number:
Japanese Patent JP6054716
Kind Code:
B2
Abstract:
PROBLEM TO BE SOLVED: To provide a method for manufacturing cyclic ethers having a high environmental friendliness capable of obtaining, without using a supercritical fluid or high-pressure reaction vessel, cyclic ethers led by isosorbide in favorable yields within brief periods and a method for recycling an ionic liquid used for the same.SOLUTION: The provided method for manufacturing cyclic ethers comprises a step of dehydrating a polyhydric alcohol possessing at least three hydroxyl groups by heating the polyhydric alcohol with microwaves by using an ionic liquid as a reaction solvent. A method for recycling the ionic liquid used for the same is also provided.

Inventors:
Akio Uemura
Koji Kaiiso
Application Number:
JP2012255324A
Publication Date:
December 27, 2016
Filing Date:
November 21, 2012
Export Citation:
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Assignee:
Yamaguchi University
Ube Industries,Ltd.
International Classes:
C07H3/10; C07D493/04
Domestic Patent References:
JP2007106685A
JP2009046429A
JP2011501729A
JP2009256347A
Foreign References:
WO2008084705A1
WO2008019219A1
US20100004437
Other References:
LI, C. et al.,Direct conversion of glucose and cellulose to 5-hydroxymethylfurfural in ionic liquid under microwave irradiation,Tetrahedron Letters,2009年,50(38),pp. 5403-5405, Supporting Information
包全喜ら,酸性イオン液体共存下におけるヘキソースからの5-ヒドロキシメチルフルフラールの製法,化学工学会第39回秋季大会 研究発表講演要旨集,2007年,Q120
Attorney, Agent or Firm:
Kisaragi International Patent Business Corporation