4,6-BIS(SUBSTITUTED)PHENYLAZORESORCINOL AND PROCESS FOR PRODUCING 4,6-DIAMINORESORCINOL

Title:

4,6-BIS(SUBSTITUTED)PHENYLAZORESORCINOL AND PROCESS FOR PRODUCING 4,6-DIAMINORESORCINOL

Document Type and Number:

WIPO Patent Application WO/2001/014319

Kind Code:

A1

Abstract:

A process for producing a 4,6-bis(substituted)phenylazoresorcinol represented by formula (2) which comprises mixing a solution of a (substituted) benzenediazonium salt represented by formula (1) with a solution or suspension of the hydroxide of an alkali metal or alkaline earth metal to obtain an alkaline mixture, mixing and reacting this mixture with an aqueous solution of resorcinol and/or of an alkali metal salt or alkaline earth metal salt thereof, and mixing the resultant reaction mixture with an acid liquid to make the mixture acid and thereby crystallize the target compound, characterized in that the acidification of the reaction mixture is conducted by adding the reaction mixture to the acid liquid and mixing them. The process is effective in reducing the time required for filtration for collecting the reaction product to thereby heighten production efficiency. (In the formulae, R represents halogeno, etc.; n is an integer of 0 to 5; and X represents chlorine, etc.).

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Inventors:

FUKUE YASUO (JP)
SHIRATORI MOTOHITO (JP)
HASHIBA ISAO (JP)
SUZUKI HIDEO (JP)

Application Number:

PCT/JP2000/005767

Publication Date:

March 01, 2001

Filing Date:

August 25, 2000

Export Citation:

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Assignee:

NISSAN CHEMICAL IND LTD (JP)
FUKUE YASUO (JP)
SHIRATORI MOTOHITO (JP)
HASHIBA ISAO (JP)
SUZUKI HIDEO (JP)

International Classes:

C07C245/08; C09B33/04; C09B41/00; C09B67/54; B01J23/02; (IPC1-7): C07C245/08; B01J23/44; C07C213/02; C07C215/80

Domestic Patent References:

WO1995023130A1	1995-08-31
WO1997016411A1	1997-05-09

Foreign References:

JPH07242604A

1995-09-19

Attorney, Agent or Firm:

Hanabusa, Tsuneo (Kandasurugadai 1-chome Chiyoda-ku Tokyo, JP)

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