Title:
APPARATUS FOR THE AUTOMATION OF CHEMICAL REACTION KINETICS STUDIES
Document Type and Number:
WIPO Patent Application WO2002077614
Kind Code:
A3
Abstract:
Disclosed is an apparatus which is capable of conducting accelerated automated kinetics studies with user-defined temperature profiles and sampling periods. The apparatus includes at least one hot reaction block for heating reaction vessels and at least one cold reaction block for cooling the reaction vessels. The apparatus includes a robotic device for transferring one reaction vessel from one hot reaction block to one cold reaction block and a controller having a user interface for inputting a predetermined temperature profile and a predetermined sampling interval. The controller is in communication with the plurality of reaction blocks and the robotic device so as to instruct the robotic device to transfer one reaction vessel from one hot reaction block to one cold reaction block at a predefined transfer time within the predetermined sampling interval.
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Inventors:
FERMIER ADAM M
OYLER ALAN R
ARMSTRONG BARBARA L
WEBER JAMES V
NALASCO JAMES
OYLER ALAN R
ARMSTRONG BARBARA L
WEBER JAMES V
NALASCO JAMES
Application Number:
PCT/US2002/008870
Publication Date:
March 27, 2003
Filing Date:
March 21, 2002
Export Citation:
Assignee:
ORTHO MCNEIL PHARM INC (US)
International Classes:
B01L7/00; G01N13/00; G01N33/15; G01N35/00; (IPC1-7): G01N13/00; G01N33/15; G01N35/00; B01L7/00
Domestic Patent References:
| WO1997016717A1 | 1997-05-09 |
Foreign References:
| FR2633310A1 | 1989-12-29 | |||
| US5964095A | 1999-10-12 |
Other References:
ZHAN X ET AL: "COMPUTER-CONTROLLED HEATING SYSTEM AND NEW COMPUTATIONN FOR RECIPROCAL HEATING STABILITY EXPERIMENT", INTERNATIONAL JOURNAL OF PHARMACEUTICS, AMSTERDAM, NL, vol. 115, no. 2, 1995, pages 167 - 173, XP001126976, ISSN: 0378-5173
ZHAN X ET AL: "DETERMINATION OF RATE ORDER FOR DEGRADATION OF DRUGS WITH NONISOTHERMAL STABILITY EXPERIMENT", JOURNAL OF PHARMACEUTICAL SCIENCES, AMERICAN PHARMACEUTICAL ASSOCIATION. WASHINGTON, US, vol. 86, no. 10, October 1997 (1997-10-01), pages 1099 - 1104, XP001126975, ISSN: 0022-3549
ZHAN X ET AL: "DETERMINATION OF RATE ORDER FOR DEGRADATION OF DRUGS WITH NONISOTHERMAL STABILITY EXPERIMENT", JOURNAL OF PHARMACEUTICAL SCIENCES, AMERICAN PHARMACEUTICAL ASSOCIATION. WASHINGTON, US, vol. 86, no. 10, October 1997 (1997-10-01), pages 1099 - 1104, XP001126975, ISSN: 0022-3549
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