Title:
FLUIDIZED BED APPARATUS AND METHOD FOR PREPARING POLYMETHOXY DIMETHYLETHER FROM METHYLAL AND PARAFORMALDEHYDE
Document Type and Number:
WIPO Patent Application WO/2015/149646
Kind Code:
A1
Abstract:
A fluidized bed apparatus and a method for preparing polymethoxy dimethylether from methylal and paraformaldehyde. The fluidized bed apparatus comprises a gas inlet (301), gas distributors (302-1, 302-2, 302-3), catalyst filling ports (303-1, 303-2, 303-3), a gas outlet (305), a fluid inlet pipe (304), catalyst discharging ports (308-1, 308-2, 308-3), a bottom component (307) and inter-sectional components (311-1, 311-2), a gas rising channel (309) of the bottom component, gas rising channels (312-1, 312-2) of the inter-sectional components, a fluid outlet (310), a downcomer (306-1) and inter-sectional downcomers (306-2, 306-3). The process for preparing polymethoxy dimethylether by using the apparatus comprises: introducing a fluidized gas from the gas inlet (301) through the gas rising channel (309) of the bottom component and the gas distributors (302-1, 302-2, 302-3) to a bottom bed layer, the gas rising to the gas outlet (305) and leaving from the fluidized bed; and introducing paraformaldehyde and methylal into the fluidized bed layer from the fluid inlet, the liquid descending to the fluid outlet (310) and leaving from the fluidized bed.
Inventors:
WANG JINFU (CN)
TANG QIANG (CN)
WANG SHENGWEI (CN)
WANG TIEFENG (CN)
CHEN SHUANGXI (CN)
WANG YUQIANG (CN)
TANG QIANG (CN)
WANG SHENGWEI (CN)
WANG TIEFENG (CN)
CHEN SHUANGXI (CN)
WANG YUQIANG (CN)
Application Number:
PCT/CN2015/075078
Publication Date:
October 08, 2015
Filing Date:
March 26, 2015
Export Citation:
Assignee:
SHANDONG YUHUANG CHEMICAL CO LTD (CN)
UNIV TSINGHUA (CN)
UNIV TSINGHUA (CN)
International Classes:
B01J8/24; B01J8/28; C07C43/30
Foreign References:
CN201768553U | 2011-03-23 | |||
CN104292085A | 2015-01-21 | |||
CN101274879A | 2008-10-01 | |||
CN101195554A | 2008-06-11 |
Attorney, Agent or Firm:
RUIBANG & PARTNERS (CN)
北京睿邦知识产权代理事务所(普通合伙) (CN)
北京睿邦知识产权代理事务所(普通合伙) (CN)
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