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Title:
FLUIDIZED BED APPARATUS AND METHOD FOR PREPARING POLYMETHOXY DIMETHYLETHER FROM METHYLAL AND PARAFORMALDEHYDE
Document Type and Number:
WIPO Patent Application WO/2015/149646
Kind Code:
A1
Abstract:
A fluidized bed apparatus and a method for preparing polymethoxy dimethylether from methylal and paraformaldehyde. The fluidized bed apparatus comprises a gas inlet (301), gas distributors (302-1, 302-2, 302-3), catalyst filling ports (303-1, 303-2, 303-3), a gas outlet (305), a fluid inlet pipe (304), catalyst discharging ports (308-1, 308-2, 308-3), a bottom component (307) and inter-sectional components (311-1, 311-2), a gas rising channel (309) of the bottom component, gas rising channels (312-1, 312-2) of the inter-sectional components, a fluid outlet (310), a downcomer (306-1) and inter-sectional downcomers (306-2, 306-3). The process for preparing polymethoxy dimethylether by using the apparatus comprises: introducing a fluidized gas from the gas inlet (301) through the gas rising channel (309) of the bottom component and the gas distributors (302-1, 302-2, 302-3) to a bottom bed layer, the gas rising to the gas outlet (305) and leaving from the fluidized bed; and introducing paraformaldehyde and methylal into the fluidized bed layer from the fluid inlet, the liquid descending to the fluid outlet (310) and leaving from the fluidized bed.

Inventors:
WANG JINFU (CN)
TANG QIANG (CN)
WANG SHENGWEI (CN)
WANG TIEFENG (CN)
CHEN SHUANGXI (CN)
WANG YUQIANG (CN)
Application Number:
PCT/CN2015/075078
Publication Date:
October 08, 2015
Filing Date:
March 26, 2015
Export Citation:
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Assignee:
SHANDONG YUHUANG CHEMICAL CO LTD (CN)
UNIV TSINGHUA (CN)
International Classes:
B01J8/24; B01J8/28; C07C43/30
Foreign References:
CN201768553U2011-03-23
CN104292085A2015-01-21
CN101274879A2008-10-01
CN101195554A2008-06-11
Attorney, Agent or Firm:
RUIBANG & PARTNERS (CN)
北京睿邦知识产权代理事务所(普通合伙) (CN)
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