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Title:
METHOD AND APPARATUS FOR SEPARATING A FLOW RICH IN CARBON DIOXIDE BY DISTILLATION TO PRODUCE LIQUID CARBON DIOXIDE
Document Type and Number:
WIPO Patent Application WO/2022/228764
Kind Code:
A1
Abstract:
In a method for separating a flow (0) containing at least 95 mol% of carbon dioxide and at least one impurity lighter than carbon dioxide by distillation, the flow (1) is cooled to a first intermediate temperature between those of the cold end and the hot end of a heat exchange means (10) in order to form a liquid flow at a first temperature and a first pressure and it is split into at least two to form a first fraction (7) and a second fraction (9), the first fraction is expanded to the pressure of a distillation column (20), referred to as second pressure, which is lower than the first pressure, and it is sent to an intermediate level of the distillation column, the second fraction is cooled in the heat exchange means to the cold end thereof, it is expanded to the pressure of the distillation column and is sent to a level of the distillation column above the point of arrival of the first fraction, a liquid flow containing at least 99 mol% of carbon dioxide is withdrawn from the bottom of the column, and a fraction (3) of the liquid flow is pressurised in a pump (PI) and sent to the top of the column.

Inventors:
TRAN MICHAEL (FR)
LECLERC MATHIEU (FR)
Application Number:
PCT/EP2022/056139
Publication Date:
November 03, 2022
Filing Date:
March 10, 2022
Export Citation:
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Assignee:
AIR LIQUIDE (FR)
International Classes:
F25J3/02; F25J3/08
Foreign References:
JPS5520206A1980-02-13
FR2975478A12012-11-23
US20130111949A12013-05-09
EP3315463A12018-05-02
US20200318897A12020-10-08
FR2100737A11972-03-24
Attorney, Agent or Firm:
MERCEY, Fiona (FR)
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