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Title:
METHOD FOR CLEANING AND DIVIDING A MIXTURE BY RECTIFICATION AND A MASS-EXCHANGE DEVICE
Document Type and Number:
WIPO Patent Application WO/2005/106368
Kind Code:
A1
Abstract:
The invention relates to cleaning and dividing a mixture by rectification process consisting in forming reflux in condensers by evaporating a coolant supplied from a storage. The inventive method consists in collecting coolant vapours in a cooling chamber for liquefying, in adding a liquid coolant to the liquefied coolant from the storage and in supplying it to the condensers for evaporation associated with a flowrate control for each condenser according to a required pressure in the contact cavity of a respective rectification tower. A chamber for receiving a stream feeding a mass-exchange device (of the rectification tower) comprises a nozzle section whose specific area is less than the specific area of a nozzle concentration part and is provided with a heater and a thermoconverter, wherein the feeding stream socket is provided with a thermal bridge. The concentration and exhaustive parts have different sizes of clear cross sections, comprise reflux distributors and redistributors which are mounted along a height from each other at a distance L=(150$m(X)300) d eq, wherein d eq is the equivalent nozzle diameter and additional perforated tubular vertical inserts are arranged in the drain holes of the bottoms of the reflux distributors and redistributors. The straight-tube pipe still of an intermediate heat carrier condenser comprises at least one channel whose cross section area is commensurable with a total area of the passage sections of heat-exchange tubes and a still electric heater has a heat-conductive base comprising an electroheating element which is placed, covered with heat conductive powder and is pressed against a still bottom by ties provided with springs. Said invention improves the reliability and reduces the coolant and metal consumption.

Inventors:
SAVINOV MIKHAIL JURIEVICH (RU)
Application Number:
PCT/RU2005/000226
Publication Date:
November 10, 2005
Filing Date:
April 27, 2005
Export Citation:
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Assignee:
SAVINOV MIKHAIL JURIEVICH (RU)
International Classes:
B01D3/00; B01D3/14; B01D3/32; B01D5/00; F25J3/02; (IPC1-7): F25J3/02; B01D3/00; B01D3/32
Foreign References:
RU2213609C12003-10-10
RU2044974C11995-09-27
RU2149676C12000-05-27
DE19526226A11997-01-23
Attorney, Agent or Firm:
Horoshkeyev, Vladimir Alexandrovich (Moscow, 8, RU)
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