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Title:
METHOD FOR MANUFACTURING NICKEL/COBALT MIXED SULFIDE FROM NICKEL OXIDE ORE BY WET SMELTING METHOD
Document Type and Number:
WIPO Patent Application WO/2020/149122
Kind Code:
A1
Abstract:
Provided is a wet smelting method whereby the amount of nickel coprecipitated with impurities is reduced and nickel yield can be increased. The present invention provides a method for manufacturing a nickel/cobalt mixed sulfide, the method including: a leaching step S1 for performing sulfuric acid leaching of a nickel oxide ore slurry under high temperature and high pressure and obtaining a leached slurry; a solid/liquid separation step S2 for separating a leaching residue from the leached slurry and obtaining a leachate including an impurity together with nickel and cobalt; a neutralization step S3 for sedimentation-separating a neutralized sediment formed by adjusting the pH of the leachate, and obtaining a neutral final liquid including nickel and cobalt; a dezincification step S4 for separating zinc and other sulfides obtained by treating the neutral final liquid with hydrogen sulfide, and obtaining a dezincified final liquid; and a nickel recovery step S5 for recovering a mixed sulfide including nickel and cobalt obtained by treating the dezincified final liquid with hydrogen sulfide; wherein the Fe(III) concentration of the neutral final liquid is adjusted to 0.18 g/L or less.

Inventors:
SUGINOHARA MAKOTO (JP)
SATO YOSHITERU (JP)
Application Number:
PCT/JP2019/050726
Publication Date:
July 23, 2020
Filing Date:
December 24, 2019
Export Citation:
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Assignee:
SUMITOMO METAL MINING CO (JP)
International Classes:
C22B23/00; C22B3/08; C22B3/22; C22B3/44
Foreign References:
JP2018059167A2018-04-12
JP2018090889A2018-06-14
JP2010037626A2010-02-18
Attorney, Agent or Firm:
TSUJIKAWA Michinori (JP)
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