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Title:
METHOD FOR PRODUCING 2-CHLOROACETOACETAMIDE
Document Type and Number:
WIPO Patent Application WO/2019/146508
Kind Code:
A1
Abstract:
A method for producing 2-chloroacetoacetamide, characterized in that acetoacetamide and trichloroisocyanuric acid are reacted in an ethanol solvent (wherein the amount of trichloroisocyanuric acid is 0.30–0.38 mol, inclusive, times the amount of acetoacetamide), the amount by weight of ethanol preferably being 3–10 times, inclusive, the amount of acetoacetamide.

Inventors:
UEKI KAZUYA (JP)
ISHIKAWA JUNICHI (JP)
Application Number:
PCT/JP2019/001383
Publication Date:
August 01, 2019
Filing Date:
January 18, 2019
Export Citation:
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Assignee:
SUMITOMO CHEMICAL CO (JP)
International Classes:
C07C231/12; C07C235/80
Foreign References:
JP2017019744A2017-01-26
JP2008120802A2008-05-29
Other References:
MARIGO, M. ET AL.: "Catalytic asymmetric bromination and chlorination of beta-ketoesters", CHEMISTRY-A EUROPEAN JOURNAL, vol. 10, no. 9, 2004, pages 2133 - 2137, XP055627323
FRINGS, M. ET AL.: "Enantioselective halogenation of E-oxo esters catalyzed by a chiral sulfoximine- copper complex", EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, vol. 24, 2009, pages 4085 - 4090, XP055627327
Attorney, Agent or Firm:
NAKAYAMA, Tohru et al. (JP)
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