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Title:
METHOD FOR PRODUCING GALLIC ACID
Document Type and Number:
WIPO Patent Application WO/2023/051745
Kind Code:
A1
Abstract:
A method for producing gallic acid, comprising the following steps: adding a tannin-containing plant crushed material to a solvent to obtain a concentrated solution containing tannic acid; adjusting the pH of the obtained concentrated solution to 3.0-7.0 by using an alkaline substance; adding tannase to the concentrated solution for hydrolysis reaction; then adding an acidic substance to adjust the pH to 1.0-3.0; cooling, crystallizing, and filtering to obtain a crude gallic acid product; heating and dissolving the obtained crude gallic acid product in purified water, and adding activated carbon to obtain a decolorized filtrate; transferring the obtained filtrate into a crystallization kettle, cooling and crystallizing, and centrifugally filtering to obtain a wet product; and drying the obtained wet product material to obtain a final gallic acid finished product having high conversion rate and high purity.

Inventors:
ZHANG HUI (CN)
ZHANG GUOXIU (CN)
XU YUANXI (CN)
DAI HONG (CN)
LI FENG (CN)
Application Number:
PCT/CN2022/122965
Publication Date:
April 06, 2023
Filing Date:
September 30, 2022
Export Citation:
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Assignee:
SHANGHAI BESTZYME BIO ENG GO LTD (CN)
NANJING BESTZYME BIO ENG CO LTD (CN)
International Classes:
C12P7/42; C07C51/42
Foreign References:
CN101864460A2010-10-20
CN112877373A2021-06-01
CN1057255A1991-12-25
US20040253694A12004-12-16
CN102643871A2012-08-22
CN106242966A2016-12-21
Attorney, Agent or Firm:
DEHEHANTONG LAW OFFICES (CN)
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