Title:
METHOD FOR PRODUCING MOLYBDENUM GRANULATED POWDER AND MOLYBDENUM GRANULATED POWDER
Document Type and Number:
WIPO Patent Application WO/2012/169257
Kind Code:
A1
Abstract:
This method for producing a molybdenum granulated powder is characterized by comprising: a step in which water is injected into a container, and heated to 50 to 80°C; a step in which a binder is added to the heated water; a step in which an aqueous solution containing molybdenum is prepared by loading molybdenum powder with an average particle size of 1 to 10 μm, to which a tin component and/or a cobalt component has been added, while stirring the water; and a step in which the aqueous solution containing molybdenum is loaded in a spray dryer in which, when the rotation speed of a rotator of the spray dryer in which the solution containing molybdenum is to be dispersed is regarded as A (rpm), and the average particle size of the granulated powder is regarded as B (μm), A/B ranges from 50 to 700, and the solution containing molybdenum is dispersed and dried to prepare a molybdenum granulated powder. The abovementioned method enables a molybdenum granulated powder having the intended average particle size, and containing a tin component and/or a cobalt component, to be efficiently produced at a high yield.
Inventors:
YAMAGUCHI SATOSHI
MORIOKA TSUTOMU
AOYAMA HITOSHI
MORIOKA TSUTOMU
AOYAMA HITOSHI
Application Number:
PCT/JP2012/057352
Publication Date:
December 13, 2012
Filing Date:
March 22, 2012
Export Citation:
Assignee:
TOSHIBA KK (JP)
TOSHIBA MATERIALS CO LTD (JP)
YAMAGUCHI SATOSHI
MORIOKA TSUTOMU
AOYAMA HITOSHI
TOSHIBA MATERIALS CO LTD (JP)
YAMAGUCHI SATOSHI
MORIOKA TSUTOMU
AOYAMA HITOSHI
International Classes:
C01B32/949; B01J2/04; B01J2/28; B22F1/14; B22F1/148; C22C27/04
Foreign References:
JP2005120400A | 2005-05-12 | |||
JP2008285759A | 2008-11-27 | |||
JPH0198764A | 1989-04-17 | |||
JPH11199948A | 1999-07-27 | |||
JP2002235141A | 2002-08-23 | |||
JPS62192556A | 1987-08-24 | |||
JPS57157447A | 1982-09-29 | |||
JP2004052020A | 2004-02-19 | |||
JP2005291530A | 2005-10-20 |
Attorney, Agent or Firm:
TOKYO INTERNATIONAL PATENT FIRM (JP)
Patent business corporation Tokyo international patent firm (JP)
Patent business corporation Tokyo international patent firm (JP)
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Claims: